CB was added in the second processing stage on the two-roll mill, with or without MLG masterbatch added at the same time. Vulcanization was performed at 300 bar with curing temperatures of 180°C for CIIR and 150°C for the other materials.

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A maximum of 75 minutes was allowed for incorporation and massing of silica. A few batches required massing on a two roll mill. After massing, a one-hour heat treatment at approximately 150-degrees-C was performed via application of high pressure steam to the jacket on the mixer. A vacuum was applied to the mixer chamber during this heat treatment.

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Inhibition of anhydride formation can occur when the fibers have 30% water by weight and are cured at 150° C. for 20 minutes. Hence, at least 30% water by weight should be present, or 30-50% water. Higher amounts of water within this range are preferred when curing at temperatures higher than 150° C., or for periods longer than 20 minutes.

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