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350 rpm with BPR (ball to powder weight ratio) 10:1 for total duration of 48 hours. The collected sample was washed with diluted HCL followed by distilled water and methanol to remove process impurities and dried in oven at 50°C for 4 hours. The dried sample (SQ9) was used for further investigations. 2.2 Characterization Techniques
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The synthesis was performed using a planetary ball mill (Fritsch PUVERISETTE 6, Germany) with 5- and 10-mm diameter milling mediain80mlZrO2 inertatmospheremillingvessel.Theelemental Ce and Si powder were loaded into milling vessel with 3:2 M ratio, with milling media of 10:1 ball-to-powder ratio. The milling pro-
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